REVIEW AND EXPERIMENTAL ON COMBINATION OF FE- PCL3 NANOPARTICLES BY MACHNOCHEMICAL DISPENSATION WITH BALL MILLING
Keywords:
Phosphorus Trichloride, Copper Nanoparticles, Ball Milling, Combination of Balls MillingAbstract
This paper reveals information on research of PCl3 nanoparticles by milling using a planetary ball mill, taking the mixture of two different sizes of balls. The milled powder is characterized using X-ray diffraction (XRD) and particles size analyzer. Samples have taken at 0, 18, 24, 30 and 40 hours after milling the powder. The crystal sizes of milled powder for different milling times are characterized. By increasing the milling time crystal size decreases. After 40 hours average crystal size of milled powder is 21nm. But controlling the size and preparation in bulk of nanoparticles eco- friendly is interesting. This paper reports on preparation of PCl3 nanoparticles by wet milling using a planetary ball mill, taking the combination of two different sizes of balls. The milled powder is characterized using X-ray diffraction (XRD) and particles size analyzer. Samples have taken at 18, 24, 36 and 50 hours after milling the powder. The crystal sizes of milled powder for different milling times are characterized. By increasing the milling time crystal size decreases. After 50 hours average crystal size of milled powder is 15nm.
There are a lot of parameters used in ball milling process. However, the parameters that have been tested most for optimization are the rotation speed and milling time. This indicates that these two parameters play an important role in determining the effectiveness of the milling. As supported by Samos, ball to powder weight ratio is recognized as one of the most influential parameters, alongside milling time and rotation speed. Zhang et al. believed that the volume of milling medium is the most influential parameter, followed by the rotation speed. The ball to powder weight ratio used by previous works clearly varies from one another. Although majority of the ratios used were in the range of 10: 1 to 20: 1, there are works that have used ratio much higher than that, going up to 100: 1 [4]. Higher ball to powder Weight ratio helps increase the particle size reduction rate. However, when the ratio used is too high, there is a possibility that contamination resulting from the collision of grinding balls and inner wall of milling vial will happen
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References
Khayati G R and Jangharban K (2012), “The nanostructure Evolution of Ag powder synthesis by high energy ball milling”, Advanced Powder Technology, Vol. 23, 393-397.
Satya V Ravikumar, Jay M Jha, Krishnayan Haldar, Surjya K Pal and Sudipto Chakraborty (2015), “Surfactant-Based Cu– Water Nanofluid Spray for Heat Transfer Enhancement of High Temperature Steel Surface” J. Heat Transfer, Vol. 137(5)102-110.
Ahmad Monshi, Mohammad Reza Foroughi and Mohammad Reza Monshi (2012), “Modified Scherrer Equation to Estimate More Accurately Nano-Crystallite Size Using XRD”, World Journal of Nano Science and Engineering, Vol. 2, 154-160.
Khayati G R and Jangharban K (2012), “The nanostructure Evolution of Ag powder synthesis by high energy ball milling”, Advanced Powder Technology, Vol. 23, 393-397.
Satya V Ravikumar, Jay M Jha, Krishnayan Haldar, Surjya K Pal and Sudipto Chakraborty (2015), “Surfactant-Based Cu–Water Nanofluid Spray for Heat Transfer Enhancement of High Temperature Steel Surface” J. Heat Transfer, Vol. 137 (5).
Ahmad Monshi, Mohammad Reza Foroughi and Mohammad Reza Monshi (2012), “Modified Scherrer Equation to Estimate More Accurately Nano-Crystallite Size Using XRD”, World Journal of Nano Science and Engineering, Vol. 2, 154-160.
Jeong W J, Kim S K and Park G C (2006), “Preparation and characteristic of ZnO thin film with high and low resistivity for an application of solar cell”, Thin Solid Films, Vol. 506-507, 180– 183
Moritz M and Geszke-Moritz M (2013), “The newest achievements in synthesis, immobilization and practical applications of antibacterial nanoparticles”, Chemical Engineering Journal, Vol. 228, 596–613.
Rekha K, Nirmala M, Nair M G, and Anukaliani A (2010), “Structural, optical, photocatalytic and antibacterial activity of zinc oxide and manganese doped zinc oxide nanoparticles,” Physica B: Condensed Matter, Vol. 405 (15), 3180–3185.
Nair S, Sasidharan A and Divya Rani V V (2009), “Role of size scale of ZnO nanoparticles and microparticles on toxicity toward bacteria and osteoblast cancer cells”, Journal of Materials Science: Materials in Medicine, Vol. 20 (1), S235–S241.
Reinert A A, Payne C, Wang L, Ciston J, Zhu Y and Khalifah P G (2013), “Synthesis and characterization of visible light absorbing (GaN) 1-x(ZnO)x semiconductor nanorods”, Inorganic Chemistry, Vol. 52 (15) 8389–8398.
Ludi B and Niederberger M (2013), “Zinc oxide nanoparticles: chemical mechanisms and classical and non-classical crystallization”, Dalton Transactions, Vol. 42 (35), 12554– 12568.
Vanmaekelbergh C and Van Vugt L K (2011), “ZnO nanowire lasers”, Nanoscale, Vol. 3 (7), 2783–2800.
Wang Z L (2004), “Zinc oxide nanostructures: growth, properties and applications”, Journal of Physics Condensed Matter, Vol. 16 (25), R829–R858.
Osmond M J and McCall M J (2010), “Zinc oxide nanoparticles in modern sunscreens: an analysis of potential exposure and hazard”, Nanotoxicology, Vol. 4 (1), 15–41.
Darvin M E, König K and Kellner-Hoeferetal M (2012), “Safety assessment by multiphoton fluorescence/second harmonic generation/hyper-Rayleigh scattering tomography of ZnO nanoparticles used in cosmetic products”, Skin Pharmacology and Physiology, Vol. 25 (4), 219–226.
Darvin M E, Haag S, Meinke M, Zastrow L, Sterry W, and Lademann J (2010), “Radical production by infrared A irradiation in human tissue”, Skin Pharmacology and Physiology, Vol. 23 (1), 40–46.
Darvin M E, Haag S F, Lademann J, Zastrow L, Sterry W and Meinke M C (2010), “Formation of free radicals in human skin during irradiation with infrared light”, Journal of Investigative Dermatology, Vol. 130 (2), 629–631.
Baroli B (2010), “Penetration of nanoparticles and nanomaterials in the skin: fiction or reality”, Journal of Pharmaceutical Sciences, Vol. 99 (1), 21–50.
Zhou G F and Bakker H, “Atomically disordered nanocrystalline Co2Si by high-energy ball milling,” Journal of Physics Condensed Matter, vol. 6, no. 22, pp. 4043–4052, 1994.
Lemine O M, Louly M A, and Al-Ahmari A.M (2010), “Planetary milling parameters optimization for the production of ZnO nanocrystalline,” International Journal of Physical Sciences, Vol.5,( 17), 2721–2729.
Nguyen T D and Do T O (2011), “Size- and Shape-Controlled Synthesis of Monodisperse Metal Oxide and Mixed Oxide Nanocrystalsed”, In Tech Publishers, Canada, 55.
Suryanarayana, (2001), “Mechanical alloying and milling,” Progress in Materials Science, vol. 46 (1-2),1–184.
Zhao W, Fang M, Wu F, Wu H, Wang L and Chen G (2010), “Preparation of graphene by exfoliation of graphite using wet ball milling”, Journal of Materials Chemistry, Vol. 20 (28), 5817– 5819.
Mahamat A, Rani A and Husain P (2012), “Behavior of Cu-WC- Ti metal composite after using planetary ball milling”, International Journal of Engineering and Applied Sciences, 278– 282.
Wang Y and Forssberg E (2006), “Production of carbonate and silica nano-particles in stirred bead milling,” International Journal of Mineral Processing, Vol. 81 (1), 1–14.
Hubert M, Petracovschi E, Zhang X H and Calvez L (2013), “Synthesisof Germanium-Gallium-Tellurium (Ge-Ga-Te) ceramics by ball-milling and sintering,” Journal of the American Ceramic Society, Vol. 96 (5), 1444–1449.
Alvarez P, Llamazares J L S and Perez M J (2008), “Microstructural and magnetic characterization of Nd2Fe17 ball milled alloys”, Journal of Non-Crystalline Solids, Vol. 354 (47– 51), 5172–5174.
Ahmeda T and Mamat O (2011), “Characterization and properties of copper-silica sand nanoparticle composites”, Defect and Diffusion Forum, Vol. 319-320, 95–105.
Esme U (2009), “Application of Taguchi method for the optimization of resistance spot welding process”, The Arabian Journal For Science and Engineering, Vol. 34 (2), 519–528.
Halim S C (2007), “Flame spray synthesis of nanoparticles for food applications: synthesis, characterization, potential hazards, cost and scalability”, Proceedings of the AIChE Annual Meeting, Salt Lake City, Utah, USA.
Guoxian L, Erde W and Zhongren W (1995), “Effects of ball- milling intensity on the amorphization rate of mixedNi50Ti50 powders”, Journal of Materials Processing Technology, Vol. 51 (1–4), 122–130.
Akcay K, Sirkecioglu A, Tatlıerb M, Savas¸O T and Erdem- S¸enatalar A (2004), “Wet ball milling of zeolite HY”, Powder Technology, Vol. 142 (2-3), 121–128.
Hedayati M, Salehi M, Bagheri R, Panjepour M and Maghzian A (2011), “Ball milling preparation and characterization of poly (ether ether ketone)/surface modified silica nanocomposite”, Powder Technology, Vol. 207 (1–3), 296–303.
Zhang D, Cai R, Zhou Y, Shao Z, Liao X Z and Ma Z F (2010), “Effect of milling method and time on the properties and electrochemical performance of LiFePO4/C composites prepared by ball milling and thermal treatment”, Electrochimica Acta, Vol. 55 (8),2653–2661.
